Experiments

  • Familiarization with the individual steps required for bioethanol production.
  • Familiarization with the plant components required for bioethanol production.
  • Study of the effect of temperature on bioethanol purity.
  • Study of the effect of pH on bioethanol yield.
  • Study of the effect of mashing time on bioethanol yield.
  • Study of the effect of fermentation time on bioethanol yield.
  • Study of the use of different raw materials to produce bioethanol.
  • Study of the effect of adding different types of yeast to the fermentation

Specification

Construction:

  • Anodized aluminum structure and panels in painted steel and HDF.
  • Main metallic elements in stainless steel.
  • This trainer includes wheels for its mobility.
  • All the vessels, valves and other accessories in contact with process materials (except the distillation unit) are made of stainless steel. The distillation unit is made of borosilicate glass. Sight glasses are made of glass.

Distillation unit:

  • Different elements made of borosilicate glass of high thermal and mechanical resistance, as well as perfect chemical inertia. It includes: A heating mantle, 1500 W.
  • Reactor flask Capacity 5L with discharge stopcock.
  • Reactor lid, with 4 inlets, especially designed for this system.
  • Vigreux type distillation column.
  • Stirring rod with stirring lock that assures a perfect insulation of the system.
  • A cold finger (dephlegmator). Liebig-West condenser with interchangeable fittings.
  • Decantation funnel of 500 ml.
  • Temperature tapings placed at key points of the system.
  • Two pump to introduce the solution into the fermentation tank and the distillation unit, range: 0-4 l./min.

Steam circuit:

1 boiler for maintain the temperature of mash tank through steam and a makeup water tank for supply of water in the boiler

Instrumentation
Temperature Sensors:

Type: K

Two temperature sensors located at the mash tank to measure the temperature of the mash inside the tank and the
temperature at the outlet of the tank’s jacket. Two temperature sensors located at the fermentation tank to measure the temperature of the preparation inside the tank and the temperature at the outlet of the tank’s jacket. Four temperature sensors located at different points of the distillation unit. One temperature sensor located at the hot water circulation system.

pH meter

Measures the pH of the mash inside the mash tank.
Range: 0~14pH

CO meter

measures the CO concentration generated during the process at the fermentation tank.
Hot water circulation system, including Pump.
Thermostatic bath.
Acid/Base circuit system, including
Industrial grade carbon monoxide detect meter
Range: 0-100%

Pumps

Two peristaltic pumps to introduce an acid or base solution into the mash tank, max. flow: 0-15 ml/min.
Two vessels to contain the acid and base solutions, volume: 1L
2 centrifugal pumps to transfer products for mash tank to fermentation tank and from fermentation tank to distillation unit. These pumps also used for backwashing the tanks with the help of directional valves.

Valves

Two motorized valves are used to divert the hot water between the jacket of the mash tank and the jacket of the fermentation tank. Six ball valves are used to drain the solution from the mash and fermentation tank or pump it into the fermentation tank and distillation unit and used for backwash of mash tank, fermentation tank and distillation tank. One ball valve is used to drain the water for hot water circulation system.

Electronic Console

Digital display for the temperature sensors
pH meter, Digital display for pH meter.
CO meter, Digital display for CO meter
Stirrers Control. 3 Switches for the stirrers (one for the mash tank, other for the fermentation tank and another for the distillation tank).

Pumps Switches

Pumps (two for the peristaltic pumps, two for the centrifugal pumps).

Heater Controls

Heating element (one for the thermostatic bath and another for the heating mantle).
Cables and Accessories, for normal operation.

Fossil fuels were used essentially for transportation, relying on the abundant and less expensive petroleum supply by then. But in the last few decades, due to the increasingly expensive petroleum supply, there has been considerable interest in the development of fuels generated from renewable resources, that is to say, biofuels. The term biofuel is attributed to any alternative fuel that derives from organic material, such as energy crops (corn, sugar, sorghum and fruits among others), crop residues or waste biomass.

Among all biofuels, ethanol has been trusted as an alternate fuel for the future, being already produced on a great scale worldwide. In this sense, bioethanol is expected to be one of the dominating renewable biofuels in the transport sector within the coming years. The Bioethanol Process trainer has been designed to perform a wide range of didactic experiments.

Various processes, such as mashing, fermentation and distillation, can be studied. The Bioethanol Process trainer has been designed to study and control the bioethanol production process on a laboratory scale. This unit allows us to monitor and examine all the important processes, from liquefaction and saccharification of the raw materials to the conversion of sugar into ethanol and distillation.

The unit consists of three main components:

  • a mash tank
  • a fermentation tank
  • a distillation unit.

 

All vessels, valves and other accessories in contact with the process materials (except the distillation unit) are made of stainless steel. The distillation unit is made of borosilicate glass. Sight glasses are made of glass. The mash tank includes an inlet at its upper cover for filling water, starch and enzymes. Its base is slightly inclined towards a port for draining the solution or pumping it into the fermentation tank. During the mashing process the starch of the raw materials is turned into glucose. The addition of the alpha-amylase enzyme enables the liquefaction of the starch slurry.

Subsequently, saccharification starts by adding the glucoamylase enzyme. A temperature sensor and a pH meter measure the properties of the mixture in the tank. The pH value is adjusted by adding acid and base. After saccharification the mash is pumped into the fermentation tank. The fermentation tank base is inclined slightly towards a port for draining the solution or pumping it into the distillation unit. The fermentation process takes place after adding yeast, producing ethanol and CO2. A temperature sensor and a CO2 meter measure the properties of the mixture and the concentration of CO2 in the tank.

Both tanks are heated indirectly with hot water through a jacket and stirred constantly. Besides, they are equipped with a sight glass so that the process can be observed and monitored. Two temperature sensors are located at the outlet of the tank’s jacket. The mash tank and the fermentation tank are thermally controlled by hot water, which is heated by a system consisting of a thermostatic bath and a pump. An additional temperature sensor is located in the thermostatic bath. After the fermentation process, the preparation is pumped into the distillation unit. It contains a heating mantle, a stirrer, a distillation column, a cold finger (dephlegmator), a condenser and a decanting funnel.